Process Engineering

Reaction Calorimetry RC1e

RC1e Application

To measures the amount of energy released (exothermic) by a Chemical reaction.
To understand the potential risk of exothermic reaction during development
To estimate the Plant scale batch cooling capacity
To understand the thermodynamics of the desired reaction, as well as that of a possible undesired reaction.

FBRM® (Focused Beam Reflectance Measurement) G600 L

FBRM Application

Direct in-process measurement with no sampling or by-pass loops required
Crystal Size Distribution Measurement and Impact of Mixing on Crystallization
Study isolated regions (fine and coarse) of the particle population
Study particles in opaque or translucent slurries and emulsions
Directly observe how process changes impact particles
Monitor particles from 0.5- 1000 μm at most process concentrations

EasyMax 102 Advanced Synthesis Workstation

EasyMax Application

Process preliminary Screening
Process optimization
Synthesis and Discovery

Radleys Reactor-Ready™ Lab Reactor (1 , 3 & 5 Lt)

Radley’s Application

To mimic plant condition and plant simulation studies
To develop robust process with respect to scale up
To study the agitation and cooling profile impact on new process
Crystallization process optimization and to meet desired physical parameter requirement.

Rapid Screening Device (RSD)

RSD Application

Thermal screening of chemical process and hazardous chemical
Multiple samples (up to 6 simultaneously)
Pressure & temperature differential measurement (simultaneously)
10mg to 100g sample
High sensitivity (detects 1% DTBP in toluene)
Thermo-kinetic quantitative data analysis
Glass, metal, reusable sample chambers

Design of Experiments (DOE)

DOE or Experimental Design is defined as the design of any information-gathering exercises where variation is present, whether under the full control of the experimenter or not. It refers to the process of planning, designing and analyzing the experiment so that valid and objective conclusions can be drawn effectively and efficiently.

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